Abstract Filling materials should be restricted to the root canal space. However, sometimes it is impossible to control the apical extrusion, in this case, the fate of the filling material and the result of the treatment will depend on its physicochemical properties and biocompatibility. Objective To evaluate the tissue response and bone repair capacity of endodontic sealers that were implanted in the calvaria of Wistar rats, forming the groups (n=16): AH Plus and Sealer Plus, compared to the clot group. Methodology On days 30 and 60, the animals were euthanized, the calvaria was removed and processed for hematoxylin-eosin, immunohistochemistry for collagen type I, Picrosirus red and microtomographic analysis. Data were subjected to ANOVA and Tuckey tests (p<0.05). Results At 30 days, all groups showed an intense inflammatory reaction (p>0.05). At 60 days, the AH Plus and Sealer Plus maintained an intense inflammatory infiltrate compared to the clot group (p<0.05). We observed immunopositive areas for type I collagen in all groups at 30 days and 60 days (p>0.05). We observed more red collagen fibers for the Sealer Plus compared to the clot group at 30 days (p<0.05). Considering the total fibers, the clot group at 30 days compared to 60 days after surgery showed an increase in the amount of matrix (p<0.05). There were no statistical differences between groups for green and yellow fibers (p>0.05). Regarding morphometric parameters, at 30 days, the newly formed bone volume and number of bone trabeculae were higher in the groups with sealers compared to the clot group (p<0.05). At 60 days, AH Plus and Sealer Plus showed greater bone neoformation compared to the clot group (p<0.05). Conclusions Despite AH Plus and Sealer Plus induced an intense inflammatory reaction, they can be considered biocompatible materials, since they allowed bone repair.

Abstract Fishburgers were made with washed mechanically separated meat (MSM) from carcass and filleting by-product (both washed and unwashed) of the Nile tilapia. The proximal composition of fishburgers was different and varied according to the raw material used, as well the color parameters. Fishburgers with MSM from filleting by-product had lower hardness and springiness, and fishburger with MSM from unwashed filleting by-product had higher yield and lower reduction in thickness. The fishburgers containing MSM from filleting by-product had better sensory acceptance, due to higher color intensities (sensory), fish odor, tenderness, succulence, cohesiveness and fish flavor. The fishburger with MSM from washed carcass was the least acceptable, because of surface uniformity. This study shows the potentiality of using MSM from tilapia filleting by-product for burgers, while the formulation of fishburgers with smaller amounts of MSM from washed carcass or with added condiments can result in improved sensory acceptance and potentiality of use.

ABSTRACT: Mechanical harvesting leaves in its wake a considerable amount of straw in the field, which can be effectively utilized to improve the soil condition and sugarcane yield. However, there is no specific information as to the quantity of straw mulch required to achieve such effects and as to whether it can be used in other sectors for bioelectricity and ethanol production. The aim of this research was to evaluate the effect of removing different amounts of straw from the field and its impact on the yield and industrial quality of sugarcane ratoons. The experiment was carried out on Rhodic soil where six treatments were evaluated including 0 %, 25 % (5 Mg ha−1), 50 % (10 Mg ha−1), 75 % (15 Mg ha−1), 100 % (20 Mg ha−1) straw on the soil surface and burned sugarcane (where 100 % of the straw was burned). The influence on yield and industrial quality was calculated using total soluble solids, Pol (Apparent sucrose content), apparent purity, total sugars, reducing sugars and fiber. Shifting the harvesting system from burned cane to growing under straw mulch improved crop yield as well as favoring sugar contents during water deficit conditions. The straw left on the soil did not affect industrial quality in any way during the trials; however, under drought conditions, treatments with 50 and 75 % of straw resulted in a 76 % higher yield compared to burned sugarcane, and 29 % more than the 0 %, 25 % to 100 % treatments of straw mulch thus favoring higher sugar production. The removal of 50 % of the straw caused no damage to the sugarcane crop.

Resumo Pães caseiros foram produzidos com quantidades de 4,4 e 4,45 g de frutanos totais por porção de 50 g, para atendimento da alegação de prebióticos, segundo a legislação brasileira. Os pães foram caracterizados, quanto ao perfil sensorial, por meio de análise descritiva, e quanto aos testes de aceitação sensorial, utilizando escala hedônica e escala do ideal para intensidade de doçura. Os perfis sensoriais dos pães mostraram-se similares, sendo a doçura o termo que discriminou os pães obtidos, visto que as intensidades diminuíram na formulação dos pães com oligofrutose/inulina para a formulação dos pães com inulina e para a formulação dos pães padrão. Comparando a cor da crosta do pão padrão com a cor da crosta do pão com inulina, o pão com inulina apresentou maior intensidade de cor bege, enquanto que o pão com oligofrutose/inulina teve menor tamanho de bolhas e maciez. O pão com oligofrutose/inulina teve maior grau de aceitação para o sabor e de forma global em relação ao pão padrão, mas as formulações dos pães com frutanos foram preferidos em relação à formulação do pão padrão para aparência, aroma, textura, sabor e aceitação global. Concluindo, a adição de frutanos em formulações de pães é promissora, podendo promover a elaboração e consumo de novos produtos prebióticos na linha de panificação.

Abstract Homemade bread was produced with 4.4 and 4.45 g of total fructans per 50 g serving to meet Brazilian standards for prebiotic claims. The bread samples were characterized for their sensory profiles using descriptive analysis and for their sensory acceptability using hedonic and just-about-right scales for sweetness intensity. The sensory profiles of the breads were similar and sweetness was the term that discriminated the bread samples obtained, since the intensity decreased from the bread formulated with oligofructose/inulin to the bread formulated with inulin and finally to the standard bread formulation. Comparing the crust colour of the standard bread with the crust colour of the bread with inulin, the bread with inulin was more beige, while the bread with oligofructose/inulin had smaller bubbles and was not as soft. The bread with oligofructose/inulin had a higher degree of acceptability with respect to flavour and overall acceptability than the standard bread, but the bread with fructans was preferred as compared to the standard bread in terms of appearance, aroma, texture, flavour and overall acceptability. In conclusion, the addition of fructans to bread formulations is promising and may promote the elaboration and consumption of new prebiotic products in the bakery line.

RESUMO: O mel de Tiúba (Melipona fasciculata) tem importância comercial na região do estado do Maranhão, no entanto a ausência de uma legislação específica para este mel entrava a ampliação de sua produção e comercialização. Dessa forma, faz-se necessário determinar as características microbiológicas e físico-químicas de méis de Tiúba, com o objetivo de fornecer subsídios para a elaboração de uma legislação específica. Assim, amostras de méis provenientes de duas bacias hidrográficas do Maranhão (Munim n = 20, e Pericumã n = 20) foram coletadas e submetidas às análises microbiológicas (coliformes totais, coliformes termotolerantes, bolores e leveduras, Clostridium sulfito redutores e Salmonella sp.) e físico-químicas (umidade, açúcares redutores e não redutores, sólidos insolúveis e solúveis, cinzas, acidez e pH). A maioria dos méis apresentou-se adequado microbiologicamente ao consumo humano, exceto uma amostra de mel proveniente de Pericumã. Os méis provenientes das duas bacias hidrográficas apresentaram diferenças em algumas características físico-químicas, o que pode ser atribuído à diversidade botânica, edáfica (solo) e climática das duas bacias. Ainda, os méis de Tiúba não se adequaram à legislação brasileira de Apis mellifera para algumas características físico-químicas, o que não permite sua regulamentação e, assim, reforça a necessidade de legislação específica para este tipo de mel.

ABSTRACT: The honey from Tiúba bees (Melipona fasciculata) is commercially important in the Brazilian state of Maranhão. However, the absence of any specific legislation for this kind of honey is an obstacle to its increased production and commercialization. Determining the microbiological and physical-chemical characteristics of different Tiúba honey can inform the elaboration of specific legislation. Thus, honey samples from two Water Catchment Areas in Maranhão (Munim and Pericumã, sample size 20 for each) were collected and submitted for microbiological analysis (total coliforms, thermotolerant coliforms, molds and yeasts, Clostridium sulfite reducers and Salmonella sp.) and physical-chemical analysis (moisture content, reducing and non-reducing sugars, insoluble and soluble solids, ash content, acidity and pH). Most of honeys sampled were suitable for human consumption, except for one sample from Pericumã. Honeys from the two water catchment areas presented differences in some physicochemical characteristics, which can be attributed to the botanic, soil and climatic diversity of the two areas. Still, these Tiúba honey samples did not fall within the Brazilian legislation for Apis mellifera honey for some of the physical-chemical characteristics, and so is not properly regulated, thus reinforcing the need for specific legislation for this type of honey.

Resumo: O objetivo deste trabalho foi avaliar o efeito de diferentes quantidades de palhada sobre o sistema radicular e a produtividade da cana-de-açúcar (Saccharum officinarum), de primeira e segunda soqueiras, em Latossolo Vermelho eutroférrico. Seis tratamentos foram avaliados : 0, 5 (25%), 10 (50%), 15 (75%) e 20 Mg ha-1 (100%) de palhada e cana-queimada, na primeira e segunda soqueiras. Utilizou-se a cana-de-açúcar 'SP80-1816'. Avaliou-se a massa de raízes a 0,45 e 0,75 m de distância da linha de plantio, até 0,60 m de profundidade. Na primeira soqueira, os tratamentos com 50, 75 e 100% de palhada proporcionaram maior massa radicular até 0,20 m de profundidade, em comparação aos tratamentos cana-queimada, 0 e 5 Mg ha-1 (25%) de palhada. Os tratamentos com 50 e 75% de palhada proporcionaram produtividades 43% maiores do que a da cana-queimada (110 Mg ha-1). O tratamento com 10 Mg ha-1 (50%) foi suficiente para proporcionar aumento da massa radicular e da produtividade da cana-de-açúcar. O sistema radicular e a produtividade da cana-de-açúcar são favorecidos pela mudança do sistema de colheita de cana-queimada para o de cana sob palhada.

Abstract: The objective of this work was to evaluate the effect of different amounts of straw on the root system and productivity of sugarcane (Saccharum officinarum), of first and second ratoons, in an Oxisol. Six treatments were evaluated: 0, 5 (25%), 10 (50%), 15 (75%), and 20 Mg ha-1 (100%) straw and burned sugarcane of the first and second ratoons. 'SP80-1816' sugarcane was used. Root mass at 0.45 and 0.75 m away from the row, and up to 0.60 m deep was evaluated. In the first ratoon, treatments with 50, 75 and 100% straw provided greater root mass up to 0.20-m depth, in comparison to treatments of burned sugarcane, and 0 and 5 Mg ha-1 (25%) straw. The treatments with 50 and 75% straw had 43% higher yields than burned sugarcane (110 Mg ha-1). The treatment with 10 Mg ha-1 straw (50%) was sufficient to provide increased root mass and productivity of sugarcane. The root system and the productivity of sugarcane are favored by the change of burned-sugarcane harvesting system to sugarcane under straw.

JUSTIFICATIVA E OBJETIVOS: A avaliação clínica de pacientes com disfunção temporomandibular inclui a avaliação da resposta dolorosa à palpação muscular e articular e existe uma incerteza sobre como a intensidade da dor relatada pelo paciente se relaciona com o limiar de dor à pressão obtido com exame de algometria. O presente estudo objetivou determinar se há uma associação entre essas duas variáveis. MÉTODOS: Oitenta pacientes com artralgia e 130 com dor miofascial mastigatória participaram deste estudo. A intensidade de dor foi aferida com a escala visual analógica. O limiar de dor à pressão foi aferido utilizando o algômetro. A pressão foi aplicada bilateralmente na articulação temporomandibular nos pacientes com artralgia e nos músculos masseter e temporal anterior. O teste utilizado na análise estatística foi o coeficiente de correlação de Pearson (r) para determinar a força da correlação entre intensidade de dor e o menor valor de limiar de dor à pressão. RESULTADOS: As correlações entre os valores de intensidade de dor e limiar de dor à pressão foram estatisticamente fracas. As correlações entre intensidade de dor e limiar de dor à pressão na articulação temporomandibular (r=-0,236; p=0,03), no masseter (r=-0,312; p<0,001) e no temporal anterior (r=-0,240; p=0,006) foram estatisticamente significantes. CONCLUSÃO: A baixa correlação entre intensidade de dor e limiar de dor à pressão sugere que outros fatores possam ser claramente importantes para explicar a experiência dolorosa de pacientes com disfunção temporomandibular, incluindo a contribuição do processo nociceptivo no sistema nervoso central e as variáveis psicossociais para a manutenção da dor crônica.

BACKGROUND AND OBJECTIVES: Physical evaluation of temporomandibular disorder patients commonly includes evaluation of pain response to muscular and articular palpation and there is a considerable uncertainty of how self-reported pain intensity relates to Pressure Pain Threshold obtained in an algometry exam. The present study aimed at determining whether pain intensity is associated to Pressure Pain Threshold in temporomandibular disorder patients. METHODS: Eighty arthralgia patients and one hundred and thirty masticatory myofascial pain patients participated in this study. Pain intensity was recorded with visual analog scale. Pressure Pain Threshold was measured using a pressure algometer. Pressure was applied bilaterally on the temporomandibular joint in arthralgia patients and masseter and anterior temporalis muscles. Pearson correlation coefficient (r) was calculated to determine the strength of the relationship between pain intensity and the lowest Pressure Pain Threshold value in each site. RESULTS: The correlation between all pain intensity and Pressure Pain Threshold values was statistically weak. Correlations between pain intensity and joint Pressure Pain Threshold (r=- 0.236; p=0.035) in the arthralgia group and pain intensity and masseter’s Pressure Pain Threshold (r=-0.312; p<0.001) and between pain intensity and anterior temporalis Pressure Pain Threshold (r=-0.240; p=0.006) were statistically significant. CONCLUSION: The weak correlation between pain intensity and Pressure Pain Threshold suggests that other factors are clearly important in explaining the pain experience of temporomandibular disorder patients, including the contribution of central nervous system nociceptive processes and psychological variables to the maintenance of chronic pain.

O mamão é um fruto cuja polpa possui características sensoriais, químicas e digestivas atrativas, apresentando alta produção no país. Apesar disso, o néctar desse fruto é pouco difundido no mercado. Assim, o presente trabalho objetivou elaborar néctares de mamão com diferentes teores de açúcar, visando a adequar a doçura ideal em açúcar para esse produto. Foram elaboradas quatro formulações de néctar de mamão, com as mesmas proporções de polpa e água, e com concentrações de açúcar a 6, 8, 10 e 12%. Cem julgadores não treinados participaram do teste afetivo de aceitação por meio da escala do ideal com nove categorias, variando de "extremamente menos doce que o ideal" a "extremamente mais doce que o ideal". Houve um aumento no percentual para a categoria "doçura ideal", conforme aumento da concentração de açúcar de 6 para 12%. Foi verificada também uma predominância na frequência de respostas para as categorias "menos doce que o ideal", para o néctar com 6% de açúcar, e para as categorias "mais doce que o ideal", para o néctar com 12% de açúcar. Para a obtenção de um néctar de mamão com "doçura ideal", a concentração de açúcar deve ser de 10,4%.

Papaya is a fruit whose pulp has attractive sensory, chemical and digestive characteristics, with high production in the country. Nevertheless, the nectar of this fruit is not widespread in the market. Thus, this study aimed to develop nectars of papaya with different sugar contents to adjust the sweetness to sugar ideal for this product. Four formulations of nectar of papaya were prepared with the same proportions of pulp and water, and sugar concentrations at 6, 8, 10 and 12%. One hundred untrained panelists participated to the affective test of acceptance by the just-about-right scale with nine categories, ranging from "extremely less sweet than ideal" to "extremely sweeter than ideal". There was an increase in the percentage for the "ideal sweetness" as sugar concentration increased from 6 to 12%. There was also verified a predominance in the frequency of responses for the categories "less sweet than ideal" to nectar of papaya with 6% sugar and for the categories "sweeter than ideal" to nectar of papaya with 12% sugar. The sugar concentration must be 10.4% to obtain nectar papaya with "ideal sweetness".

Existem diversos estudos que propõem mudanças na tecnologia de vinificação para melhorar a qualidade do vinho tinto, refletindo na sua maior aceitabilidade. Nesse contexto, o objetivo do presente artigo foi avaliar a influência da pré-secagem e da remontagem constante na aceitabilidade dos vinhos tintos das cultivares Bordô (Ives) e Isabel quanto aos atributos aparência, aroma, corpo, sabor e à impressão global (aceitação global). Oitenta consumidores avaliaram as amostras utilizando uma escala hedônica estruturada de 9 pontos e uma escala de intenção de compra de 5 pontos. Os dados hedônicos foram analisados por meio da Análise de Cluster e Escalonamento Multidimensional. Diferenças significativas (P<0.001) foram observadas na comparação das amostras em todos os atributos sensoriais, destacando a grande aceitação das amostras elaboradas pelas técnicas inovadoras. Adicionalmente, a Análise de Cluster mostrou com sucesso a segmentação da preferência dos consumidores, mostrando a relevante aceitação dos vinhos dos tratamentos de pré-secagem e bagaço estático. A correlação entre o sabor e a aceitação global foi significativa (P<0.001; r>0.700), mostrando que o sabor exerce grande influência na avaliação global das amostras de vinho, independentemente dos outros atributos. A relevante aceitação global dos vinhos dos tratamentos inovadores sugere o grande potencial desses processos de vinificação.

Several studies proposed changes in winemaking technology in order to improve wine quality, reflecting on its high acceptance. Thus, the aim of this work was to evaluate the influence of pre-drying and constant pumping effect technologies on sensory attributes of Bordô (Ives) and Isabel red wines through the acceptance evaluation of appearance, aroma, body, flavor and overall acceptance. Eighty consumers evaluated the samples using a 9-point structured scale and sensory data were analyzed by Cluster Analysis followed by Multidimensional Scaling. Significant differences (P<0.001) were observed in the comparison of the samples in all sensory attributes, highlighting the wide acceptance of the samples from innovative winemaking. In addition, Cluster Analysis showed the split of consumer preferences which revealed the higher preference and purchase intention of the pre-drying and static pomace wines. The correlation between flavor and overall acceptance was significant (P<0.001; r>0.700) and the consumer panel showed that the overall acceptance of the wines was influenced by the flavor, regardless of the other attributes. The higher acceptance of the pre-drying and static pomace wines suggests the potential of these winemaking processes.

O objetivo neste trabalho foi estimar as exigências de lisina digestível e de energia metabolizável (EM) para codornas de corte (Coturnix coturnix sp) em crescimento. Foram utilizadas 1.680 codornas de 4 a 35 dias de idade, não-sexadas, em delineamento experimental inteiramente casualizado em esquema fatorial 4 × 4 (LD = 0,92; 1,12; 1,32 e 1,52% × EM = 2.800; 2.900; 3.000 e 3.100 kcal/kg de ração), totalizando 16 dietas, avaliadas com 3 repetições de 35 codornas por unidade experimental. O aumento dos níveis de lisina digestível na ração provocou aumento linear do peso corporal, do ganho de peso, do consumo de lisina e do rendimento de peito e redução do teor de água nos cortes. Quando houve aumento dos níveis de energia metabolizável na ração, observou-se redução linear no consumo de lisina e aumento do peso corporal e do rendimento de gordura abdominal. O aumento simultâneo dos níveis de lisina e energia metabolizável na ração, no entanto, provocou redução linear no consumo de ração e melhora linear da conversão alimentar no período de 4 a 35 dias, mas aumentou o teor de gordura nos cortes. A exigência nutricional de lisina digestível para máximo crescimento de codornas de corte é maior ou igual a 1,52%. O nível de 2.800 kcal/kg de EM na ração é suficiente para bom desempenho das aves, contudo, para melhor conversão alimentar, são necessário níveis mais elevados.

The objective of this experiment was to estimate the digestible lysine and metabolizable energy (ME) requirements for growing meat quails (Coturnix coturnix sp). A total of 1,680 quails from 4 to 35 days of age of both sexes were used in a complete random experimental design in a 4 × 4 factorial scheme (DL = 0.92; 1.12; 1.32 and 1.52% × ME = 2,800; 2,900; 3,000 and 3,100 kcal/kg of the ration) totaling 16 diets evaluated with 3 replications of 35 quails per experimental diet. Increase of the levels of digestible lysine in the diet linearly increased body weight, weight gain, lysine intake and breast yield and reduced water content in the cuts. When levels of metabolizable energy were increased in the diet, it was observed a linear reduction on consumption of lysine and an increase of body weight and abdominal fat yield. However, The simultaneous increase of levels of lysine and metabolizable energy in the diet linearly reduced feed intake and linearly improved feed conversion in the 4-35 day period, but it increased fat content in the cuts. The nutritional requirement of digestible lysine for maximum growth of meat quails is greater than or equal to 1.52%. The level of 2,800 kcal/kg ME in ration is sufficient to allow a good performance of the birds, however, for a better feed conversion, greater levels are needed.

The volatile compounds of raw and extruded bovine rumen, extracted by dynamic headspace, were separated by gas chromatography and analyzed by GC-MS. Raw and extruded materials presented thirty-two volatile compounds. The following compounds were identified in raw bovine rumen: heptane, 1-heptene, 4-methyl-2-pentanone, toluene, hexanal, ethyl butyrate, o-xylene, m-xylene, p-xylene, heptanal, limonene, nonanal, dodecane, tridecane, tetradecane, pentadecane, hexadecane, heptadecane and octadecane. The following compounds were identified in the extruded material: 1-heptene, 2,4-dimethylhexane, toluene, limonene, undecane, tetradecane, pentadecane, hexadecane, heptadecane, octadecane and nonadecane. Mass spectra of some unidentified compounds indicated the presence of hydrocarbons with branched chains or cyclic structure.