In order to analyze the effect of the growth direction on dendrite arm spacing (λ1) and microhardness (HV) during horizontal directional solidification (HDS), experiments were carried out with the Al-3wt.%Cu-5.5wt.%Si alloy and the results compared with others from the literature elaborated for upward directional solidification (UDS). For this purpose, a water-cooled directional solidification experimental device was developed, and the alloy investigated was solidified under unsteady-state heat flow conditions. Thermal parameters such as growth rate (VL) and cooling rate (TR) were determined experimentally and correlations among VL, TR, λ1 and HV has been performed. It is observed that experimental power laws characterize λ1 with a function of VL and TRgiven by: λ1=constant(VL)-1.1 and λ1=constant(TR)-0.55. The horizontal solidification direction has not affected the power growth law of λ1 found for the upward solidification. However, higher values of λ1 have been observed when the solidification is developed in the horizontal direction. The interrelation of HV as function of VL, TR and λ1 has been represented by power and Hall-Petch laws. A comparison with the Al-3wt.%Cu alloy from literature was also performed and the results show the Si element affecting significativaly the HV values.

Nesse trabalho, a transição colunar/equiaxial (TCE) foi investigada experimentalmente na solidificação unidirecional de três ligas multicomponentes à base de alumínio (Al-nSi-3Cu), com “n” igual a 5,5, 7,5 e 9% em massa. Os principais parâmetros analisados foram o gradiente de temperatura (GL), a velocidade de deslocamento da isoterma liquidus (VL), a taxa de resfriamento (TR) e a composição de Si. Um dispositivo de solidificação direcional refrigerado à agua para fluxo de calor transitório foi utilizado. Para todas as ligas examinadas, os resultados mostram que a concentração de soluto inflencia na posição da TCE, a qual ocorre para uma taxa de resfriamento igual a 1.17 0C/s. A análise comparativa entre os resultados desse trabalho com os da literatura, propostos para analizar a TCE em ligas Al-Si, é conduzida e os resultados mostram que o final da região colunar acontece para uma taxa de resfriamento sete vezes maior que a encontrada para ligas Al-Si.

In this work the columnar to equiaxed transition (CET) was experimentally investigated in the unidirectional solidification of three aluminum based multicomponent alloys (Al-nSi-3Cu), with "n" equal to 5.5, 7.5 and 9 wt.%. The main parameters analyzed include the tip temperature gradient (GL), tip growth rate (VL), tip cooling rate (TR) and Si content. A water-cooled solidification experimental setup was developed, and specimens were solidified under unsteady state heat flow conditions. It is shown that for the alloys examined, the solute concentration influences the position of the CET, which occurs for an average cooling rate of about 1.17 0C/s. A comparative analysis between the results of this work and those from literature proposed to analyze the CET during upward vertical solidification of Al-Si alloys is reported and the results show that the end of the columnar region is abbreviated as a result of seven times higher critical cooling rate than that verified for Al-Si alloys.

O principal objetivo desse trabalho é investigar a influência dos parâmetros térmicos velocidade de solidificação (V L) e taxa de resfriamento (T R), nos espaçamentos dendríticos primários (λ1) da liga hipoeutética Al-7%Si, durante a solidificação direcional horizontal, em regime transiente. Os valores de λ1 foram medidos ao longo do comprimento do lingote e correlacionados com esses parâmetros. A variação dos espaçamentos dendríticos estudados é expressa por meio de funções na forma de potência de V Le T Rdadas, respectivamente, por λ1= 55(V L)-1.1e λ1= 212 (T R)-0.55. Um estudo comparativo é realizado entre os resultados encontrados nesse trabalho e aqueles obtidos para a mesma liga quando solidificada direcionalmente nos sistemas verticais ascendente e descendente, sob as mesmas condições assumidas. Finalmente, os resultados experimentais obtidos são comparados com valores fornecidos por alguns modelos teóricos propostos na literatura para analisar espaçamentos dendríticos primários.

The main purpose of this work is to investigate the influence of thermal parameters such as growth rate (V L) and cooling rate (T R) on the primary dendrite arm spacings (λ1) during the horizontal transient directional solidification of Al-7wt.%Si hypoeutectic alloy. The primary dendrite spacings were measured along the length of the samples and correlated with these thermal parameters. The variation of dendrite spacings is expressed as a power law function of V L and T R given by the formulas λ1 = 55(V L)-1.1 and λ1 = 212 (T R)-0.55, respectively. A comparative study between the results of this work and those from the literature proposed to investigate these dendrite spacings during the upward and downward vertical directional solidification of Al-7wt.%Si alloy is also conducted. Finally, the experimental data are compared with some predictive dendritic models from the literature.