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Article • J. Braz. Chem. Soc. 22 (1) • Jan 2011 • https://doi.org/10.1590/S0103-50532011000100011   copy

Synthesis and characterization of a linker for primary amines used in the solid phase organic synthesis of spermidine

Authorship SCIMAGO INSTITUTIONS RANKINGS

A linker resin for the synthesis of functionalized spermidine in good yield is described, along with its characterization by infrared (IR), 13C solid-state nuclear magnetic resonance with cross polarization and magic angle spinning (13C CPMAS NMR) and ¹H high resolution magic angle spinning nuclear magnetic resonance (¹H HRMAS NMR. This linker has been regenerated after cleavage of spermidine and re-used without loss of efficiency.

polyamines; 13C CPMAS NMR; HRMAS NMR; solid phase organic synthesis; spermidine

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