1 |
126.9 s |
- |
126.1 s |
- |
126.6 s |
- |
2 |
130.2 s |
- |
130.9 s |
- |
131.0 s |
- |
3 |
144.0 s |
- |
143.4 s |
- |
144.1 s |
- |
4 |
148.0 s |
- |
150.2 s |
- |
147.3 s |
- |
5 |
113.8 d |
6.80 (d, 1H, J 8.5, Ph-H) |
113.0 d |
6.87 (d, 1H, J 8.5, Ph-H) |
113.6 d |
6.81 (d, 1H, J 8.5, Ph-H) |
6 |
120.0 d |
7.42 (d, 1H, J 8.5, Ph-H) |
120.2 d |
7.47 (d, 1H, J 8.5, Ph-H) |
120.0 d |
7.43 (d, 1H, J 8.5, Ph-H) |
1' |
114.2 s |
- |
114.9 s |
- |
114.6 s |
- |
2' |
164.5 s |
- |
164.1 s |
- |
164.2 s |
- |
3' |
102.9 d |
6.37 (d, 1H, J 2.2, Ph-H) |
103.9 d |
6.37 (d, 1H, J 2.2, Ph-H) |
102.7 d |
6.38 (d, 1H, J 2.2, Ph-H) |
4' |
168.5 s |
- |
166.1 s |
- |
168.2 s |
- |
5' |
107.6 d |
6.45 (dd, 1H, J 8.8, 2.2, Ph-H) |
108.7 d |
6.49 (dd, 1H, J 8.8, 2.2, Ph-H) |
107.3 d |
6.48 (dd, 1H, J 8.8, 2.2, Ph-H) |
6' |
133.1 d |
8.08 (d, 1H, J 8.8, Ph-H) |
133.1 d |
8.09 (d, 1H, J 8.8, Ph-H) |
133.1 d |
8.04 (d, 1H, J 8.8, Ph-H) |
1" |
25.3 t |
3.60 (d, 2H, J 6.8, CH2) |
25.2 t |
3.60 (d, 2H, J 6.8, CH2) |
23.2 t |
3.43 (d, 2H, J 6.8, CH2) |
2" |
124.0 d |
5.14 (t, 1H, J 6.8, CH) |
123.9 d |
5.13 (t, 1H, J 6.8, CH) |
123.2 d |
5.21 (t, 1H, J 6.8, CH) |
3" |
132.0 s |
- |
132.0 s |
- |
134.5 s |
- |
4" |
26.0 q |
1.63 (s, 3H, CH3) |
25.9 q |
1.68 (s, 3H, CH3) |
68.9 t |
3.96 (s, 2H, CH2) |
5" |
18.0 q |
1.83 (s, 3H, CH3) |
17.9 q |
1.85 (s, 3H, CH3) |
14.3 q |
1.68 (s, 3H, CH3) |
a |
119.2 d |
7.65 (d, 1H, J 15.1, CH) |
119.4 d |
7.63 (d, 1H, J 15.1, CH) |
119.1 d |
7.62 (d, 1H, J 15.1, CH) |
b |
143.2 d |
8.18 (d, 1H, J 15.1, CH) |
143.0 d |
8.19 (d, 1H, J 15.1, CH) |
143.0 d |
8.20 (d, 1H, J 15.1, CH) |
C=O |
192.3 s |
- |
192.5 s |
- |
192.5 s |
- |
4-OMe |
- |
- |
55.9 q |
3.80 (s, 3H, CH3) |
- |
- |
4'-OMe |
56.0 q |
3.80 (s, 3H, CH3) |
- |
- |
56.0 q |
3.80 (s, 3H, CH3) |
3-OH |
- |
12.83 (s, 1H, OH) |
- |
12.88 (s, 1H, OH) |
- |
12.85 (s, 1H, OH) |
4-OH |
- |
12.51 (s, 1H, OH) |
- |
- |
- |
12.50 (s, 1H, OH) |
2'-OH |
- |
13.17 (s, 1H, OH) |
- |
13.45 (s, 1H, OH) |
- |
13.18 (s, 1H, OH) |
4'-OH |
- |
- |
- |
13.66 (s, 1H, OH) |
- |
- |