Qui-1 |
4.77 (d, J = 8.0 Hz) |
103.2 |
|
4.75 (d, J = 8.0 Hz) |
103.0 |
2 |
4.44 (dd, J = 9.0, 8.0 Hz) |
77.1 |
|
4.45 (dd, J = 9.0, 8.0 Hz) |
76.8 |
3 |
4.33 (dd, J = 9.0, 9.0 Hz) |
79.6 |
|
4.33 (t, J = 9.0, 9.0 Hz) |
79.4 |
4 |
3.63 (dd, J = 9.0, 9.0 Hz) |
78.0 |
|
3.65 (dd, J = 9.0, 9.0 Hz) |
77.7 |
5 |
3.67 (dq, J = 9.0, 6.0 Hz) |
73.2 |
|
3.67 (dq, J = 9.0, 6.0 Hz) |
72.9 |
6 |
1.59 (d, J = 6.0 Hz) |
19.7 |
|
1.61 (d, J = 6.0 Hz) |
19.1 |
Rha-1 |
5.89 (brs) |
100.4 |
|
5.88 (brs) |
100.2 |
2 |
4.79 (dd, J = 3.0, 2.0 Hz) |
70.7 |
|
4.80 (dd, J = 3.0, 2.0 Hz) |
70.5 |
3 |
5.76 (m*) |
79.7 |
|
5.75 (t, J = 8.8 Hz) |
79.5 |
4 |
4.32 (dd, J = 9.9, 9.9 Hz) |
86.1 |
|
4.33 (dd, J = 9.9, 9.9 Hz) |
85.9 |
5 |
4.83 (dq, J = 9.9, 6.5 Hz) |
68.9 |
|
4.84 (dq, J = 9.6, 6.5 Hz) |
68.6 |
6 |
1.92 (d, J = 6.5 Hz) |
19.3 |
|
1.93 (d, J = 6.5 Hz) |
19.3 |
Rha'-1 |
5.64 (brs) |
99.9 |
|
5.64 (brs) |
99.8 |
2 |
5.88 (dd, J = 3.0, 2.0 Hz) |
74.3 |
|
5.88 (dd, J = 3.0, 2.0 Hz) |
73.9 |
3 |
4.15 (m*) |
81.9 |
|
4.34 (dd, J = 9.0, 3.0 Hz) |
79.4 |
4 |
3.66 (dd, J = 9.9, 9.9 Hz) |
75.9 |
|
3.68 (dd, J = 9.9, 9.9 Hz) |
75.6 |
5 |
3.86 (dq, J = 9.9, 6.5 Hz) |
72.6 |
|
3.85 (dq, J = 9.9, 6.5 Hz) |
72.3 |
6 |
1.49 (d, J = 6.5 Hz) |
18.8 |
|
1.49 (d, J = 6.5 Hz) |
18.6 |
Fuc-1 |
5.29 (d, J = 7.6 Hz) |
107.1 |
|
5.30 (d, J = 7.6 Hz) |
106.9 |
2 |
4.33 (dd, J = 9.2, 7.6 Hz) |
74.2 |
|
4.33 (dd, J = 9.6, 7.6 Hz) |
73.7 |
3 |
4.25 (dd, J = 9.2, 3.0 Hz) |
80.9 |
|
4.25 (dd, J = 9.2, 3.0 Hz) |
81.7 |
4 |
5.63 (brs) |
74.9 |
|
5.64 (brs) |
74.7 |
5 |
3.93 (q, J = 6.0 Hz) |
70.9 |
|
3.93 (q, J = 6.0 Hz) |
70.7 |
6 |
1.32 (d, J = 6.4 Hz) |
17.7 |
|
1.31 (d, J = 6.4 Hz) |
17.4 |
conv-1 |
|
173.2 |
|
|
|
2a |
2.82 (ddd, J = 10.4, 7.6, 2.0 Hz) |
35.2 |
|
|
|
2b |
2.43 (ddd, J = 10.4, 7.6, 2.0 Hz) |
|
|
|
|
11 |
3.79-3.82 (m*) |
81.7 |
|
|
|
14 |
0.90 (t, J = 7.2 Hz) |
14.8 |
|
|
|
jal-1 |
|
|
|
|
173.0 |
2a |
|
|
|
2.88 (ddd, J = 16.4, 10.4, 6.0 Hz) |
35.6 |
2b |
|
|
|
2.43 (ddd, J = 16.4, 10.4, 6.0 Hz) |
|
11 |
|
|
|
3.82-3.88 (m*) |
80.9 |
16 |
|
|
|
0.85 (t, J = 6.8 Hz) |
14.7 |
tga-1 |
|
168.2 |
|
|
168.0 |
2 |
|
129.7 |
|
|
129.4 |
3 |
6.99 (dq, J = 7.2, 1.6 Hz) |
138.3 |
|
6.99 (dq, J = 7.2, 1.6 Hz) |
138.0 |
4 |
1.49 (d, J = 7.2 Hz) |
14.9 |
|
1.49 (d, J = 7.2 Hz) |
14.6 |
5 |
1.85 (brs) |
13.1 |
|
1.81 (brs) |
12.7 |
tga'-1 |
|
169.0 |
|
|
169.0 |
2 |
|
129.6 |
|
|
129.3 |
3 |
7.13 (dq, J = 7.2, 1.2 Hz) |
138.8 |
|
7.13 (dq, J = 7.2, 1.2 Hz) |
138.5 |
4 |
1.47 (d, J = 7.2 Hz) |
15.1 |
|
1.45 (d, J = 7.2 Hz) |
14.5 |
5 |
1.87 (brs) |
13.0 |
|
1.86 (brs) |
12.7 |