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Impact Response of Aluminium Alloy Foams Under Complex Stress States

Abstract

A series of dynamic tests were conducted on a closed-cell aluminum alloy foams in order to determine experimental failure surface under impact loading conditions. Quasi-static tests have also been performed to investigate failure mechanism under different stress paths. Three typical types of deformation modes can be observed, which corresponds to the different failure mechanism. The failure loci of the foam in principal stress plane are explored from quasi-static to dynamic loading conditions. A significant strength enhancement is identified experimentally. The expansion of the failure locus from the quasi-static to the dynamic test is almost isotropic. A modified failure criterion for the metallic foam is proposed to predict failure locus as a function of strain rate. This rate-dependence failure criterion is capable of giving a good description of the biaxial failure stresses over a wide range of the strain rates.

Keywords:
Metallic Foams; Impact loading; Failure mode; Dynamic failure surface

1 INTRODUCTION

Sandwich structures are widely used in various engineering applications such as protective structures of autos and aircrafts, due to their excellent energy absorption capability, high specific strength and superior shock-resistance characteristics under such extreme loading as blast or ballistic impact (Ashby et al, 2000; Lu and Yu, 2003Lu, G., Shen, J., Hou, W., Ruan, D., Ong LS., (2008). Dynamic indentation and penetration of aluminium foams. International Journal of Mechanical Sciences 50:932-943.; Gibson and Ashby, 1997Gibson, L.J., Ashby, M.F. (1997). Cellular solids, structure and properties, Cambridge University Press.; Djamaluddin et al, 2015Djamaluddin, F., Abdullah, S., Ariffin, A.K., Nopiah, Z.M.,(2015). Multi objective optimization of foam-filled circular tubes for quasi-static and dynamic responses. Latin American Journal of Solids and Structures 12:1126-1143.). Metallic foams as well as the other cellular materials are used increasingly in engineering applications such as energy absorbers and the cores of sandwich panels due to superior properties like high specific strength, high specific stiffness and high energy dissipation capacity. In these applications, metallic foams may be subjected to multiaxial loadings. The deformation modes and the macroscopic stress distributions are non-uniform under combined stress states. Therefore, it is necessary to develop an understanding of mechanical properties for metallic alloy foams under multiaxial stress states. The goal of the present study is to model accurately the mechanical behavior of the aluminum alloy foam under different stress paths, especially multiaxial impact loading conditions.

Many previous works have been performed to investigate the multiaxial behavior of commercially available foams ranged from polymer-based foams to metal-based foams. (Gibson et al., 1989Gibson, L.J., Ahsby, M.F., Zhang, J., Triantafillou T.C., (1989). Failure surfaces of cellular materials under multiaxial loads-I. Modelling. International Journal of Mechanical Sciences 31:635-663.) experimentally studied several failure mechanisms such as elastic buckling, plastic collapse and brittle fracture for cellular solids under multiaxial loading conditions, and further suggested a failure criterion for ideal cellular solids. (Deshpande and Fleck, 2000aDeshpande, V.S., Fleck, N.A., (2000) a. Isotropic constitutive models for metallic foams. Journal of the Mechanics and Physics of Solids 48:1253-1283.) investigated experimentally the failure behavior of aluminum alloy foams under a range of axisymmetric compressive and hydrostatic stress states. Two phenomenological constitutive models were proposed to characterize multiaxial failure behavior of the metallic foams. In addition, a series of axisymmetric compressive and tensile tests on the polymer foams have been performed in order to further verify two constitutive models (Deshpande and Fleck, 2001Deshpande, V.S., Fleck, N.A., (2001). Multi-axial yield behaviour of polymer foams. Acta Materialia 49:1856-1866.). (Gioux et al., 2000Gioux, G., McCormack, T.M., Gibson, L.J., (2000). Failure of aluminium foams under multiaxial loads. Journal of the Mechanics and Physics of Solids 42:1097-1117.) carried out experimental works on both closed-cell aluminum alloy foams (Alporas) and open-cell aluminum alloy foams (Duocel) under axisymmetric triaxial and biaxial loading condition to verify various published theoretical failure criteria. (Doyoyo and Wierzbicki, 2003Doyoyo, M., Wierzbicki, T., (2003). Experimental studies on the yield behaviour of ductile and brittle aluminium foams. International Journal of Plasticity 19:1195-1214.) modified the standard Arcan apparatus (Arcan et al., 1978Arcan, M., Hashin, Z., Voloshin, A., (1978). Method to produce uniform plane stress states with applications to fiber-reinforced materials. Experimental Mechanics 18:141-146.) for investigating experimentally biaxial response of ductile and brittle aluminum foams. A phenomenological failure criterion is presented to predict the measured failure surfaces for Alporas and Hydro closed-cell aluminium foams. (Ruan et al., 2007Ruan, D., Lu, G., Ong, L.S., Wang, B., (2007). Triaxial compression of aluminium foams. Composites Science and Technology 67:1218-1234.) employed a custom-built triaxial testing apparatus to investigate the effect of strain rate in the experimental failure surface of CYMAT closed-cell aluminum foams. Recently, (Combaz et al., 2010aCombaz, E., Bacciarini, C., Charvet, C.R., Dufour, W., Dauphin, F., (2010) a. Yield surface of polyurethane and aluminium replicated foam. Acta Materialia 58:5168-5183., 2011Combaz, E., Bacciarini, C., Charvet, C.R., Dufour, W., Mortensen, A., (2011). Multiaxial yield behaviour of Al replicated foam. Journal of the Mechanics and Physics of Solids 59:1777-1793.) used a triaxial testing device to perform a series of multiaxial experiments on replicated aluminum foam. They proposed that the shape of the measured failure surface for the replicated aluminum foams depended on the third stress tensor invariant.

The aforementioned literatures related to the multiaxial behavior of the foams have been focused on quasi-static failure surface and failure criterion. The deformation modes and failure mechanism under different combined stress states, which is closely related to constitutive property of the foams, have not been experimentally investigated as yet. Hence, this paper presents dynamic and quasi-static biaxial tests for a closed-cell aluminum alloy foam with two objectives in mind. The first objective is to study the deformation modes of the foam under different combined stress states, and to further investigate the failure mechanism. On the other hand, the metallic foams have been used extensively as energy absorbers to resist impact loads due to their high energy absorption capacity. Therefore, it is essential to model accurately the multiaxial failure behavior of the metallic foams under impact loading conditions, especially combined shear-compression which is the most realistic loading mode. The previous researches involving the dynamic mechanical property of the foams have been mostly limited to the uniaxial mechanical behavior, such as uniaxial failure strength, the plateau stress, the densification behavior and the energy absorption capacity (Zhao, 1997Zhao, H., (1997). Testing of polymeric foams at high and medium strain rates. Polymer Testing 16:507-516.; Deshpande and Fleck, 2000bDeshpande, V.S., Fleck, N.A., (2000) b. High strain rate compressive behaviour of aluminium alloy foams. International Journal of Impact Engineering 24:277-298.; Zhou et al., 2004aZhou, J., Shrotriya, P., Soboyejo, W.O., (2004a). Mechanisms and mechanics of compressive deformation in open-cell Al foams. Mechanics of Materials 36:781-97.; Zhou et al., 2004bZhou, J., Gaob, Z., Cuitinob, A., Shrotriya, P., (2004b). Effects of heat treatment on the compressive deformation behavior of open cell aluminum foams. Materials Science and Engineering A 386:118-128.; Demiray et al., 2006Demiray, S., Becker, W., Hohe, J., (2006). Analysis of two-and three-dimensional hyperelastic model foams under complex loading conditions. Mechanics of Materials 38, 985-1000.; Doyoyo and Mohr., 2006Doyoyo, M., Mohr, D. (2006). Experimental determination of the mechanical effects of mass density gradient in metallic foams under large multiaxial inelastic deformation. Mechanics of materials, 38(4), 325-339.; Yu et al., 2006Yu, J.L., Li, J.R., Hu, S.S., (2006). Strain-rate effect and micro-structural optimization of cellular metals. Mechanics of Materials 38:160-170.; Peroni et al., 2008Peroni, L., Avallea, M., Peroni, M., (2008). The mechanical behaviour of aluminium foam structures in different loading conditions. International Journal of Impact Engineering 35: 644-658.; Peroni et al., 2012Peroni, L., Scapina, M., Avallea, M., Weiseb, J., Lehmhusc, D., (2012). Dynamic mechanical behavior of syntactic iron foams with glass microspheres. Materials Science and Engineering A 552:364-375.; Zhou et al., 2012aZhou, Z.W., Wang, Z.H., Zhao, L.M., Shu, X.F., (2012a). Experimental investigation on the yield behavior of Nomex honeycombs under combined shear-compression. Latin American Journal of Solids and Structures 9:515-530., 2012bZhou, Z.W., Wang, Z.H., Zhao, L.M., Shu, X.F., (2012b). Loading rate effect on yield surface of aluminum alloy foams. Materials Science and Engineering A 543:193-199., 2014Zhou, Z.W., Wang, Z.H., Zhao, L.M., Shu, X.F., (2014). Uniaxial and biaxial failure behaviors of aluminium alloy foams. Composites Part B: Engineering 61:340-349.; Hangai et al., 2013Hangai, Y., Kubota, N., Utsunomiy, T., Kawashima, H., Kuwazuru, O., Yoshikawa, N., (2015). Drop weight impact behavior of functionally graded aluminum foam consisting of A1050 and A6061 aluminum alloys. Materials Science and Engineering A 639:597-603.; Pichler and Lackner, R., 2013Pichler, C., Lackner, R., (2013). Sesqui-power scaling of plateau strength of closed-cell foams. Materials Science and Engineering A 580:313-323.; Duarte et al., 2014Duarte, I., Vesenjak , M., Krstulović-Opara, L., (2014). Variation of quasi-static and dynamic compressive properties in a single aluminium foam block. Materials Science and Engineering A 616:171-182.; Kaya and Fleck, 2014Kaya, A.C., Fleck, C., (2014). Deformation behavior of open-cell stainless steel foams. Materials Science and Engineering A 615: 447-456.; Li et al., 2014Li, Z.Q., Zhang, J.J., Fan, J.H., Wang, Z.H., Zhao, L.M., (2014). On crushing response of the three-dimensional closed-cell foam based on Voronoi model. Mechanics of Materials 68:85-94.; Alvandi-Tabrizi et al., 2015Alvandi-Tabrizi, Y., Whisler, D.A., Kim, H. , Rabiei, A.,(2015). High strain rate behavior of composite metal foams. Materials Science and Engineering A 631:248-257.; Storm et al., 2015Storm, J., Abendroth, M., Kuna, M., (2015). Influence of curved struts, anisotropic pores and strut cavities on the effective elastic properties of open-cell foams. Mechanics of Materials 86:1-10.; Vesenjak et al., 2016Vesenjak, M., Sulong, M. A., Krstulović-Opara, L., Borovinšek, M., Mathier, V., & Fiedler, T., (2016). Dynamic compression of aluminium foam derived from infiltration casting of salt dough. Mechanics of Materials 93, 96-108.). But experimental investigations of metallic foams under dynamic multiaxial loading condition are not available by now. The main reason for such situations lies in the difficulties to carry out dynamic multiaxial experiments because of the requirements for both a feasible multiaxial design in a tiny limited space and an accurate data measurement under impact conditions. Therefore, the second goal of this paper is to investigate experimentally biaxial mechanical behavior of the metallic foams under impact conditions, and to further determine the dynamic failure surface of the metallic foams. Based on the dynamic results, a rate-dependence failure criterion is proposed to predict the failure surface as a function of strain rate for the foam. Moreover, the size effect and the anisotropic behavior for the closed-cell aluminum alloy foam were also experimentally investigated in this paper.

2 MATERIALS AND TESTING PROCEDURES

2.1 Materials and Samples

The material under investigation is the closed-cell aluminum alloy foam manufactured by the China Shipbuilding Industry Corporation (CSIC). A typical electron microscope photograph of this foam microstructure is shown in Figure 1. The manufacturers' data shows that the chemical composition of the matrix materials (cell wall) is AL-0.45 wt.%Mg-0.52 wt.%Ca-0.21 wt.%Ni. It has a nominal density of 2710 kg/m3, Young's modulus of 70.2 GPa and yield strength of 192 MPa. The density of this aluminum alloy foam is 0.405g/cm3, corresponding to the mean relative density of 15%, which is defined as the density of the foam blocks divided by the density of the cell-wall material. It is worth emphasizing that the relative density of the foam samples used in tests has variation value of ±0.8% relative to the mean value. The main reason such situation is the variation of cell diameter. The cell diameter of the closed-cell foam has a range of value from 1 mm to 4.5 mm, corresponding to the mean diameters of 2.4 mm. In this paper, all foam samples were fabricated with high precision to minimize damage of the local cell wall. Electrical Discharge Machining method (EMD) was adopted to obtain the foam samples. All foam samples were cut from rectangular foam blocks with dimension of 1500 mm ×500 mm ×100 mm supplied by the manufacturers.

Figure 1
Scanning electron micrograph of closed-cell aluminum alloy foam.

2.2 Sample Sizes

Previous researches reveal that commercial metal foams generally exhibit anisotropic mechanical properties (Gibson and Ashby, 1997Gibson, L.J., Ahsby, M.F., Zhang, J., Triantafillou T.C., (1989). Failure surfaces of cellular materials under multiaxial loads-I. Modelling. International Journal of Mechanical Sciences 31:635-663.; Andrews et al., 1999Andrews, E., Sanders, W., Gibson, L.J., (1999). Compressive and tensile behaviour of aluminum foams. Materials Science and Engineering A 270:113-124.; Chen et al., 2001Chen, C., Fleck, N.A., Lu, T.J., (2001). The mode I crack growth resistance of metallic foams. Journal of the Mechanics and Physics of Solids 49:231-259.; Alkhader and Vureal, 2009Alkhader, M., Vural, M., (2009). The partition of elastic strain energy in solid foams and lattice structures. Acta Materialia 57:2429-2439.; Combaz et al., 2010bCombaz, E., Rossoll, A., Mortensen, A., (2010b). Hole and notch sensitivity of aluminium replicated foam. Acta Materialia 59:572-581.; Marie and David, 2013Marie, E.C., David, C.D., (2013). Anisotropic mechanical properties of amorphous Zr-based foams with aligned, elongated pores. Acta Materialia 61:5937-5948.). Thus, uniaxial compression tests are first conducted on cubic sample with the dimension of 40mm in three mutually perpendicular principal directions (shown in Figure 2) in order to characterize directional properties of this foam, which should be taken into consideration before investigating mechanical behavior. On the other hands, it is well-known that mechanical behavior of metallic foam is strongly sensitive to the ratio of the sample size to the cell size at length scales where the two are of the same order of magnitude (Bastawros et al., 2000Bastawros, A.F., Bart, S.H., Evans, A.G., (2000). Experimental analysis of deformation mechanisms in a closed-cell aluminum alloy foam. Journal of the Mechanics and Physics of Solids 48:301-322.; Onck et al., 2001Onck, P.R., Andrews, E.W., Gibson, L.J., (2001). Size effects in ductile cellular solids. Part I: Modeling. International Journal of Mechanical Sciences 43:681-699.; Andrews et al., 2001Andrews, E.W., Gioux, G., Onck, P.R., Gibson, L.J., (2001). Size effects in ductile cellular solids. Part II: Experimental results. International Journal of Mechanical Sciences. 43:701-713.; Jeon and Asahina, 2005Jeon, I., Asahina, T., (2005). The effect of structural defects on the compressive behavior of closed-cell Al foam. Acta Materialia 53:3415-3423.; Joseph et al., 2005Joseph, F. R., Anthony, M. Waas., (2005). Size effects and the shear response of aluminum foam. Mechanics of Materials 37:69-82.; Rakow and Waas, 2005Rakow, J. F., Waas, A. M. (2005). Size effects and the shear response of aluminum foam. Mechanics of Materials 37, 69-82.; Tekoğlu and Onck, 2008Tekoğlu, C., Onck, P.R., (2008). Size effects in two-dimensional Voronoi foams: a comparison between generalized continua and discrete models. Journal of the Mechanics and Physics of Solids 56:3541-3564.; Caner and Bazant, 2009Caner, F. C., Bazant, Z. P., (2009). Size effect on strength of laminate-foam sandwich plates: Finite element analysis with interface fracture. Composites Part B: Engineering 40:337-348.; Jeon et al., 2009Jeon, I., Katou, K., Sonoda, T., Asahina, T., Kang, K. J., (2009). Cell wall mechanical properties of closed-cell Al foam. Mechanics of Materials 41, 60-73.; Tekoğlu et al., 2011Tekoğlu, C., Gibson, L.J., Pardoen, T., Onck, P.R., (2011). Size effects in foams: experiments and modeling. Progress in Materials Science 56:109-138.; Su et al., 2014Su, B.Y., Zhou, Z.W., Wang, Z.H., Li, Z.Q., Shu, X.F., (2014). Effect of defects on creep behavior of cellular materials. Materials Letters. 136: 37-40.). Most researchers have adopted big size samples in the mechanical tests to avoid the size effect of cellular materials (McCullough et al., 1999McCullough, K.Y.G., Fleck, N.A., Ashby, M.F., (1999). Toughness of aluminium alloy foams. Acta Materialia 47:2323-2330.; Ruan et al., 2002Ruan, D., Lu, G., Chen, F.L., Siores, E., (2002). Compressive behaviour of aluminium foams at low and medium strain rates. Composites Structure 57:331-336.; Saha et al., 2005Saha, M.C., Mahfuz, H., Chakravarty, U.K., Uddin, M., Kabir, M.E., Jeelani, S., (2005). Effect of density, microstructure, and strain rate on compression behavior of polymeric foams. Materials Science and Engineering A 406:328-336.; Amsterdam et al., 2008Amsterdam, E., Hosson, J.T.M.D., Onck P.R., (2008). On the plastic collapse stress of open-cell aluminum foam. Scripta Materialia 59: 653-656.; Lu et al., 2008Lu, G., Shen, J., Hou, W., Ruan, D., Ong LS., (2008). Dynamic indentation and penetration of aluminium foams. International Journal of Mechanical Sciences 50:932-943.; Shen et al., 2010Shen, J.H., Lu, G.X., Ruan, D., (2010). Compressive behaviour of closed-cell aluminium foams at high strain rates. Composites Part B: Engineering 41:678-685.; Mangipudi and Onck, 2011Mangipudi, K.R., Onck, P.R., (2011). Tensile failure of two-dimensional quasi-brittle foams. Acta Materialia 59:7356-7367.; Luong et al., 2013Luong, D. D., Pinisetty, D., Gupta, N., (2013). Compressive properties of closed-cell polyvinyl chloride foams at low and high strain rates: Experimental investigation and critical review of state of the art. Composites Part B: Engineering 44, 403-416.; Jin et al., 2015Jin, T., Zhou, Z.W., Wang, Z.H., Wu, G.Y., Shu, X.F., (2015). Experimental study on the effects of specimen in-plane size on the mechanical behavior of aluminum hexagonal honeycombs. Materials Science and Engineering A 635:23-35.). Thus, In order to ensure the accuracy of the experimental results in this paper, size effect of this foam in mechanical behavior was experimentally studied first. The uniaxial compression tests were carried out on cubic foam samples with different dimensions by using Instron testing machine (Model 5544, Instron,) with a 2 kN load cell. The dimensions of the sample include 5 mm, 9 mm, 13 mm, 17 mm, 21 mm, 25 mm, 30 mm and 40 mm, respectively. The foam samples were carefully prepared using an arrangement, as showed in Figure 3. The uniaxial compression tests were conducted by controlling the constant vertical displacement rate of 0.02mm/s, corresponding to a nominal strain rate of 5.0 × 10-4s-1. In the previous works, the ratio of samples size to cell size L/d was introduced to analyse the size effect in the mechanical behavior of metallic foam (Onck et al., 2001Onck, P.R., Andrews, E.W., Gibson, L.J., (2001). Size effects in ductile cellular solids. Part I: Modeling. International Journal of Mechanical Sciences 43:681-699.; Tekoğlu et al., 2011Tekoğlu, C., Gibson, L.J., Pardoen, T., Onck, P.R., (2011). Size effects in foams: experiments and modeling. Progress in Materials Science 56:109-138.). For the sake of illustration convenience, the ratio of the sample length to cell size of L/d is also used in subsequent analysis.

Figure 2
Foam samples used in tests for investigation of anisotropic properties.

Figure 3
Foam samples with different dimensions

2.3 Dynamic Multiaxial Loading Device and Testing Procedures

The Split-Hopkinson pressure bar is nowadays a popular impact loading setup for studying the dynamic compressive behavior of materials. Initially developed for metallic material testing, it has now been used for many different materials such as polymer materials, geotechnical materials and biological material. A typical Split-Hopkinson pressure bar device consists of long input and output bars with a short sample placed between them. A projectile launched by a gas gun strikes the free end of the input bar and creates a compressive longitudinal incident wave εi (t). Once this wave arrives at the bar-sample interface, part of it εr (t), is reflected, whereas the other part passes through the sample and transforms into the transmitted wave εt (t) in the output bar. Two gauges are fixed at the middles of input and output bars to collect those experimental data (incident, reflected and transmitted waves) which should be adopted to deduced the forces and the velocities at both faces of the sample and further determinate dynamic constitutive behavior of testing materials.

Figure 4
Dynamic multiaxial loading tests.

In order to realize multiaxial dynamic loading, two short cylindrical bars with one bevel end are inserted at the interfaces of the samples and impact-bars, as illustrated in Figure 4. The two short cylindrical bars have the same diameter of 37mm as the input and output bars. The Hopkinson bars and the two short beveled bars are both made of the pure aluminium. The main purpose for this design is to ensure that the incident wave transmits from the input bar to the input beveled bar are not reflected significantly, and the transmitted wave can also propagate from the out-put beveled bar to the output bar completely. The foam sample is inserted at the two parallel bevels instead of contacting with the input and output bars directly and perpendicularly. A square sleeve made of Teflon is applied to support the multiaxial dynamic loading device, and further make sure the only horizontal movement of the beveled bars in whole loading process. It should be pointed out that the friction coefficient between the foam sample and the beveled bars should be large enough to insure that no slippage occurs during multiaxial loading process. In this way, when the foam sample is loaded by multiaxial dynamic loading device, a multiaxial stress state is realized. A series of multiaxial tests on the aluminum alloy foam were performed at the impact velocity of about 10 m/s with the loading angles ranging from 0º (corresponding to the uniaxial compression for a strain rate of 1100s-1) to 60º.

Instead of adopted Split-Hopkinson pressure bar data processing method which deduced directly to average stress-strain curve base on the assumption of homogeneous stress-strain field of sample in whole loading process, here traditional Split-Hopkinson pressure bar device is only used as loading and measuring system. According to the stress wave theory, the stress and the particle velocity of a single wave can be directly deduced from the associated strain recorded by strain gauges at the input and output bars. Moreover, these collected strain signals are not only known at the points of strain gauges, but at any point on the input and output bars. Thus, forces and velocities at the interfaces of the bar/samples can be deduced by the local strain signals shifted from the recording points. The associated forces and particle velocities at the interfaces of the bar/samples are then calculated as follows:

(1)

(2)

(3)

(4)

Where Finput, Foutput, Vinput and Voutput are forces and particle velocities on bar/samples faces. Sb, E and C 0 are respectively the cross section area, elastic modulus of the bars and the longitudinal wave speed. Εi (t), εr (t), εt (t) are the recorded strain signals collected from the points of strain gauges on the input and output bars.

Since a stress/strain homogeneous field assumption is not really applicable in this multiaxial loading case of the foam sample with localized deformation mechanism, The mean pressure P(t) as a function of the overall crush D(t) is introduced to gives an overall prediction of the multiaxial behavior of this closed-cell aluminum alloy foam under impact loadings. Based on above deductions of the forces and velocities, the mean pressure P(t) and the overall crush, D(t) (with the same definition as in the quasi-static case) are calculated as follows:

(5)

(6)

Where Ss is the area of the sample face contacting to the beveled bars.

2.4 Quasi-static Multiaxial Loading Tests

In order to further study multiaxial behavior of the foam under different stress path, quasi-static multiaxial loading tests were performed at different loading angles by using a universal material testing machine with a 10 kN load cell, as shown in Figure 5. The tests were conducted by controlling the constant vertical displacement rate of 0.02 mm/s and the vertical pressure-displacement curves were acquired with computer.

Figure 5
Quasi-static multiaxial loading tests.

Figure 6
Multiaxial stress state of foam sample.

Figure 7
Displacement boundary condition of foam sample

The main goal of quasi-static multiaxial tests is to investigate the multiaxial deformation mode and failure mechanisms, and to further determine the quasi-static failure surface of the foam. Therefore, the stress states of the foam sample in testing process will be analyzed in detail. As the stiffness of the cylindrical bars with one bevel is much higher than the stiffness of the foam sample, the cylindrical bars are assumed to be rigid in the subsequent analysis. The mean shear stress and the mean normal stress of the foam sample are defined in a local coordinate system, where the x-axis is perpendicular and the y-axis is parallel to the interfaces of the bar/samples (Figure 6). The force along the positive axis of the universal testing machine is defined as the vertical force Fy . The force perpendicular to the vertical one is referred to as the horizontal forceFr , which is the constraining force exerted on the cylindrical bars by the sleeve. For the sake of illustration convenience, the angle between the loading direction (vertical direction) of the universal testing machine and the axial direction of the foam sample is referred to as the loading angle, as shown in Figure 6. Clearly, the larger the loading angle is, the more dominant the shear component is. When 0 = 0º, the uniaxial tests is achieved. According to the global static equilibrium, the vertical force and the constraining force in the cylindrical bars can be given by following expressions:

(7)

(8)

WhereLis the length of cubic sample. Based on above analysis, a uniform displacement field (Sx,Sy ) at the top interfaces of the foam sample can be defined as to be displacement boundary conditions, as shown in Figure 7.

(9)

(10)

The proportional loading path is determined by the multiaxial loading angle.

(11)

The kinematically admissible displacement field of the foam sample in whole loading process can be obtained:

(12)

(13)

Since small deformations of the foam sample in elastic stage, the strain in the local x-direction, x, the strain in the local y-direction, y, and the shear distortion, Yxy can be calculated as follows:

(14)

(15)

(16)

The isotropic material law that establishes the stress-strain relationship under plane-stress conditions is introduced in this multiaxial loading state:

(17)

In Eq. (17), [Cij ] denotes the stiffness matrix of an isotropic lamina in plane stress conditions. v is the Poisson's ratio of the foams,E is the Young's modulus. Eq. (17) can be used to relate the strain and stress ratios as:

(18)

According to Eq. (7) to (18), the shear stress and compressive stress of the foam sample in the elastic phase (as shown in Figure 6) can be expressed in following equations:

(19)

(20)

(21)

Figure 8
Uniaxial compressive stress-stain curves for different loading directions.

3 RESULTS AND DISCUSSIONS

3.1 Isotropic Behavior of the Foams

All macroscopic stress-strain curves in uniaxial compression tests are based on the engineering stress and strain definition. The stress versus strain responses on the cubic samples with dimension of 40mm are shown in Figure 8. The shape of the stress-strain curves is typical of metallic foams, including an increase up to a peak stress, then a drop to a stage of more or less constant stress, finally an increase rapid to a densification stage. The stress-strain curves obtained from different loading directions are consistent well. In other words, this aluminum alloy foams exhibit obviously isotropic properties.

3.2 Determination of the Sample Dimension

The stress-strain curves on the cubic samples with different dimensions are shown in Figure 9. The shape of the curves is similar for all samples, but the actual values of the stiffness and the strength varied. The main goal of this section is to investigate the size effect in the mechanical properties, rather than to describe the mechanism of the size effect. The dimension of the cubic sample used in multiaxial tests can be further determined. Therefore, the initial failure stress and the plateau stress of the sample are taken into consideration in subsequent analysis. The initial failure stress of the foam, corresponds to the collapse of the weakest layer of foam cells, is defined by the peak stress of the uniaxial stress-strain curve. The plateau stress is defined by an energy efficiency method (Li et al., 2006Li, Q.M., Magkiriadis, I., Harrigan, J.J., (2006). Compressive strain at the onset of the densification of cellular solids. Journal of Cellular Plastics 42:371-392.). Energy absorption efficiency η(εa ) is defined as the energy absorbed up to a given nominal strain Ea normalized by the corresponding stress value σc(ε).

(22)

Densification strain εD is the strain value corresponding to the stationary point in the efficiency-strain curve where the efficiency is a global maximum, i.e.

(23)

The plateau stress σpl , can then be calculated by

(24)

Figure 9
Uniaxial compressive stress-stain curves for foam samples with different sizes.

A typical energy absorption efficiency curve for the foam, illustrating the densification strain and the plateau stress, is shown in Figure 10. It is shown that energy absorption efficiency increases with the compressive strain up to the maximum value, while decreases when strain exceeds the densification strain.

Figure 10
Stress-strain curve and energy absorption efficiency-strain curve of the foam.

The initial failure stress and the plateau stress are plotted against the foam sample sizeLrelative to the cell sized, as shown in Figure 11. The initial failure stress increases with increasing normalized sample size up to a plateau level at L/d = 7,08. This testing result closely agrees with the conclusions of (Andrews et al., 2001Andrews, E.W., Gioux, G., Onck, P.R., Gibson, L.J., (2001). Size effects in ductile cellular solids. Part II: Experimental results. International Journal of Mechanical Sciences. 43:701-713.) in terms of the increasing initial failure stress with increasing L/d > 6 for the closed-cell foam. The difference is that the growth rate is somewhat faster for this foam. The plateau stress follows a similar pattern, increasing with L/d up to a plateau level at L/d = 7,08. Therefore, it can be clearly concluded that in order to obtain the bulk mechanical properties of this aluminum alloy foam, a block of sizes L/d > 6 is necessary. Thus, the cubic sample with the dimension of 17mm is adopted in the multiaxial tests.

Figure 11
Initial failure stresses and plateau stresses plotted against normalized sample edge length.

3.3 Multiaxial Behavior of the Foam During Quasi-static Tests.

The quasi-static pressure-displacement curves of the foams at different loading angles are summarized in Figure 12. For these multiaxial results, the following observation can be made: In the elastic region, the vertical pressure versus displacement curve is initially linear, but becomes non-linear at the following short stages due to the loss of stiffness caused by the progressive crushing of cells. This behavior continues until the peak pressure is achieved, after which the load drops. The slope of the curve and the initial peak pressure decreases with the increase of loading angle θ, which represents that the stiffness and strength mechanism is strongly sensitive to the stress path (loading angle).

Figure 12
Vertical pressure-displacement curves for different loading angles.

In an effort to show how crushing evolved through the entire process of loading, the deformation process of the sample corresponding to points on the curves were captured by camera under the different loading angles. For the cases of small loading angles such as 10º, the whole crushing process of the foam is similar to the results observed in uniaxial compression due to the stress state dominated by compressive stress. First, the peak pressure represents the initial plastic buckling of the weakest layer in the foams. Subsequently, deformation will be localized within this layer until these cells were fully compacted and the next series of cells starts to collapse (as shown in Figure 13).

Figure 13
Images for deformation process and the associated pressure history for 10º foam sample.

For the cases of large loading angle such as 60º, the initial plastic collapse area appeared in side of the samples, as shown in Figure 14. Subsequently, an inclined crushing band spread from one side to other side of the samples, which is clearly illustrated by the global images from 3 to 6 in Figure 14. Finally, this crushing band further propagated, and a single crack across the whole sample gradually formed, which correspond to images 5 in Figure 14. It should be noted that the crack band had a 3D distribution in the whole foam since the crushed band is also inclined in a plane perpendicular to the original one. Therefore, the side view of the sample is illustrated in Figure 15.

Figure 14
Images for deformation process and the associated pressure history for 60º foam sample.

Figure 15
Side view of 60º foam sample.

It is clearly seen that there is no obvious crushing area except for a fracture band across the whole sample. The main reason for this fracture is that shear stress plays important role in deformation mode. In other words, as that the shear displacement is more than the normal displacement under this proportional path, the failure mode of the sample in the cases of large loading angles is dominated by shear stress.

For the cases of loading angle θ = 40º, the cell area in the top surface of the sample initially started to plastic collapse, as shown in Figure 16. The deformation process of localized crushed bands from the initial plastic collapse area to the side of the sample, rather than across the whole sample, is observed. Finally, a single crack band further formed along the initial crush bands, and meanwhile the cell layer near the top surface of the sample is successive crushed. It means that two deformation modes competitively exist in the post-peak stage due to the shear stress. Furthermore, the shear stress and the normal stress both play a fairly role in deformation process under this stress path. It is worthwhile to emphasize that the deformation processes captured by images reveal no obvious slippage between the sample and the bevels at the elastic stage for all loading angles. As evidenced by the global images from Figures 13 to 16, that is to say the analysis for the displacement boundary (shown in section 2.4) is reliable at the elastic stage.

Figure 16
Images for deformation process and the associated pressure history for 40º foam sample.

3.4 Multiaxial Behavior of the Foam During Dynamic Tests

Examples of the dynamic pressure-displacement responses for the foams at different loading angles are illustrated in Figure 17. It can be found that the level of the dynamic curve strongly depends on loading angle, which is consistent to the quasi-static results. For example, the slope of the curve before reaching the peak pressure decreases with the increase of loading angle θ. The peak pressure also decreases with the increase of loading angle θ, implying much easier initial failure of the foams at larger loading angle. The average level of the pressure plateau becomes lower as the loading angle increases. On the other hand, the differences between quasi-static and dynamic results are summarized. The quasi-static curves are smoother than the dynamic curves. The initial peak values of quasi-static curves are not as significant as the corresponding dynamic results for all loading angles, and the slopes of the elastic stages in each curves are much larger than the quasi-static results. Finally, as observed from the plateau level of each curve, the quasi-static curves are all lower than the corresponding dynamic ones, which indicated a significant effect of the strain rate.

Figure 17
Dynamic pressure-displacement curves for different loading angles.

For quantitatively illuminating the enhancement from quasi-static to dynamic results, the initial peak pressure and the plateau pressure will be analyzed in following section. The plateau pressure is defined as follows:

(25)

Where Smax is the maximum displacement of the corresponding crushing duration. The peak pressure and the plateau pressure at different loading angles for dynamic and quasi-static cases are plotted in Figure 18. It is evident that the peak pressure and the plateau pressure of the foams under dynamic conditions is significantly higher than the results under quasi-static conditions. A notable strength enhancement is concluded from the dynamic to the quasi-static results.

Figure 18
Peak pressures and Plateau pressures in quasi-static and dynamic multiaxil tests.

3.5 Determination of Dynamic Failure Surface

Many works have been performed to study the rate effect in the mechanical behavior of the metallic foams, such as the uniaxial failure stress, the plateau stress, the densification behavior and the energy absorption capacity (Zhao,1997Zhao, H., (1997). Testing of polymeric foams at high and medium strain rates. Polymer Testing 16:507-516.; Deshpande and Fleck, 2000bDeshpande, V.S., Fleck, N.A., (2000) b. High strain rate compressive behaviour of aluminium alloy foams. International Journal of Impact Engineering 24:277-298.; Demiray et al., 2006Demiray, S., Becker, W., Hohe, J., (2006). Analysis of two-and three-dimensional hyperelastic model foams under complex loading conditions. Mechanics of Materials 38, 985-1000.; Yu et al., 2006Yu, J.L., Li, J.R., Hu, S.S., (2006). Strain-rate effect and micro-structural optimization of cellular metals. Mechanics of Materials 38:160-170.; Zhou et al., 2012aZhou, Z.W., Wang, Z.H., Zhao, L.M., Shu, X.F., (2012a). Experimental investigation on the yield behavior of Nomex honeycombs under combined shear-compression. Latin American Journal of Solids and Structures 9:515-530., 2012bZhou, Z.W., Wang, Z.H., Zhao, L.M., Shu, X.F., (2012b). Loading rate effect on yield surface of aluminum alloy foams. Materials Science and Engineering A 543:193-199., 2014Zhou, Z.W., Wang, Z.H., Zhao, L.M., Shu, X.F., (2014). Uniaxial and biaxial failure behaviors of aluminium alloy foams. Composites Part B: Engineering 61:340-349.; Castroa et al., 2013Castroa, G., Nutt, S.R., Wenchen, X.,(2013). Compression and low-velocity impact behavior of aluminum syntactic foam. Materials Science and Engineering A 578: 222-229.; Alia et al., 2014Alia, R.A., Cantwell, W.J., Langdon, G.S., Yuen, S.C.K., Nurick, G.N., (2014). The energy-absorbing characteristics of composite tube-reinforced foam structures. Composites Part B: Engineering 61:127-135.; Goel et al., 2014Goel, M.D., Matsagar, V.A., Gupta, A.K., (2014). Blast resistance of stiffened sandwich ranels with closed-cell aluminum foam. Latin American Journal of Solids and Structures 11:2497-2511.; Li et al., 2014Li, Z.Q., Zhang, J.J., Fan, J.H., Wang, Z.H., Zhao, L.M., (2014). On crushing response of the three-dimensional closed-cell foam based on Voronoi model. Mechanics of Materials 68:85-94.; Wang et al., 2014Wang, L., Yang, X., Zhang, J., Zhang, C., He, Li., (2014). The compressive properties of expandable microspheres/epoxy foams. Composites Part B: Engineering 56:724-732.; Kishimoto et al., 2014Kishimoto, S., Wang,Q., Tanaka, Y., Kagaw, Y., (2014). Compressive mechanical properties of closed-cell aluminum foam-polymer composites. Composites Part B: Engineering 64:43-49.; Caprino et al., 2015Caprino, G., Durante, M., Leone, C., Lopresto, V.,(2015). The effect of shear on the local indentation and failure of sandwich beams with polymeric foam core loaded in flexure. Composites Part B: Engineering 71:45-51.; Storm et al., 2015Storm, J., Abendroth, M., Kuna, M., (2015). Influence of curved struts, anisotropic pores and strut cavities on the effective elastic properties of open-cell foams. Mechanics of Materials 86:1-10.; Su et al., 2015Su, B.Y., Zhou, Z.W., Zhang, J.J., Wang, Z.H., Shu, X.F., Li, Z.Q., (2015). A numerical study on the impact behavior of foam-cored cylindrical sandwich shells subjected to normal/oblique impact. Latin American Journal of Solids and Structures 12:2045-2060.). Nevertheless, little literature has involved the experimental failure surface, especially the dynamic failure surface which is very important for the engineering applications of the metallic foams. Therefore, the multiaxial failure stresses obtained from quasi-static to dynamic tests are plotted in principal stress plane in order to probe the failure surface of the aluminum alloy foams over a wide range of the strain rates, as shown in Figure 19. It is clearly found that the significant expansion of experimental failure locus from low to high strain rates is almost isotropic, even though the normal stress/shear stress ratio for a given loading angle is same under quasi-static and dynamic loading conditions.

Generally speaking, the mechanisms of rate sensitivity of the metallic foams may be attributed to the effects of intrinsic length scale of the material, the rate sensitivity of base material, the compression and flow of gas in cells, micro-structural morphology including the form, shape, size of the individual cell and other effects such as inertia effect, which may cause to different deformation modes of the material at high strain rate cases. On the other hand, the mechanical properties of commercial metallic foams usually have variations of ±5% from the mean value as highly heterogeneity of materials. Based on aforementioned considerations, we adopt the criterion of a 20% increase in failure stress to define the strain rate sensitivity. It is consistent with the fact that the metallic foams are highly heterogeneous materials with scatter strength of the order of 20% (Deshpande and Fleck, 2000bDeshpande, V.S., Fleck, N.A., (2000) b. High strain rate compressive behaviour of aluminium alloy foams. International Journal of Impact Engineering 24:277-298.). It can be found that over the range of the strain rates investigated, the foams exhibit an obviously strain rate dependence in the uniaxial failure stress and the experimental failure surface. This multiaxial data can be used to further determinate the rate-dependent constitutive model of the aluminum alloy foams which is very useful for the impact cases. (Miller, 2000Miller, R.E., (2000). A continuum plasticity model for the constitutive and indentation behaviour of foamed metals. International Journal of Mechanical Sciences 42:729-754.) developed to a continuum plasticity framework for the cellular material and other types of materials exhibiting plastic compressibility base on the Drucker-Prager criterion for soil:

(26)

Where p is the hydrostatic compressive stress, σc is the uniaxial compressive strength, σe is the von Mises equivalent stress. The constants γ, α' and d 0 are related to the uniaxial strength and the plastic Poisson's ratio. To characterize the rate-dependent failure behavior of the aluminum alloy foams, uniaxial compressive stresses of the foams from low to high strain rates are plotted in Figure 20 (Zhou et al., 2014Zhou, Z.W., Wang, Z.H., Zhao, L.M., Shu, X.F., (2014). Uniaxial and biaxial failure behaviors of aluminium alloy foams. Composites Part B: Engineering 61:340-349.). Based on the present uniaxial data, the empirical formula can be determined to describe uniaxial compressive strength as function of the strain rates:

(27)

Where A and p is material parameters related to the strain rate sensitivity. Based on the fitted uniaxial stress contours shown in Figure 20 (Zhou et al., 2014Zhou, Z.W., Wang, Z.H., Zhao, L.M., Shu, X.F., (2014). Uniaxial and biaxial failure behaviors of aluminium alloy foams. Composites Part B: Engineering 61:340-349.), the values of A and p can be determined as 1.95 and 0.067.

Figure 19
Failure surfaces of the aluminum alloy foams at different strain rates.

Figure 20
Uniaxial failure stressses of the aluminum alloy foams at different strain rates.

The comparison between the experimental failure locus and the modified Miller criterion is made in Figure 19. It can be seem that the rate-dependent failure criterion gives a good description of the multiaxial failure behavior of this aluminum alloy foams from the quasi-static loading to the dynamic loading. It means that the dynamic failure surface for this foam might be derived by using the enhancing ratio of uniaxial compressive strength and the quasi-static failure surface.

4 CONCLUSIONS

Two different types of tests, i.e. uniaxial compression test, multiaxial test, have been conducted on the closed-cell aluminum alloy foams in this paper. Uniaxial compressive tests were first carried out to investigate the anisotropic property of the foam and the size effect of the sample in mechanical behaviors. The foam exhibits isotropic mechanical property. To obtain the bulk mechanical properties of this foam, the sample size L/d > 6 is necessary. Multiaxial tests have been performed on the foam over a wide range of strain rates in order to study multiaxial failure behavior under combined stress paths. The strength and stiffness of the foam are strongly sensitive to stress path (loading angle). Three types of typical deformation pattern of the foam were observed, which corresponds to the different failure mechanisms. A notable enhancement of the initial failure pressure and the plateau pressure is clearly found from the quasi-static to the dynamic results. The failure loci of the foams in principal stress plane were determinated experimentally over a wide range of the strain rates. The expansion of the failure locus from the quasi-static to the dynamic conditions is almost isotropic. A modified failure criterion was proposed to predict the failure locus of the metallic foams as a function of strain rate. This rate-dependence failure criterion is capable of giving a good description of the experimental failure stresses for this foam over a wide range of the strain rates. More dynamic data under different multiaxial loading conditions should be collected to further confirm the proposed rate-dependent failure criterion, which is still on the way.

Acknowledgements

This work is supported by the Natural Science Foundation of China (Grant Nos. 11172195). The financial contributions are gratefully acknowledged.

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Publication Dates

  • Publication in this collection
    Apr 2016

History

  • Received
    05 Aug 2015
  • Reviewed
    04 Nov 2015
  • Accepted
    15 Dec 2015
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